Temperature calibration in the cooling operation mode
of the UNIPAN-TERMAL 605 M model DSC calorimeter (English version)
Polimery 2000, No 9, 614
SummaryA method  of temperature calibration of the differential scanning calorimeter operated in the cooling mode is described on the example of a UNIPAN-TERMAL 605 M DSC instrument. Such a calibration is important in studying the nonisothermal crystallization of materials that crystallize at a slow rate, e.g., polymers. The result of measurement is shown to be related to the rate of temperature change and to sample mass. Application of extraneous coolant, e.g., liquid nitrogen, leads to an additional effect.